TOTAL SUSPENDED SOLIDS (TSS)
Principle :A well-mixed sample is filtered through a weighed standard filter paper and dried to a constant weight at 103oC to 105oC.The increase in weight of the filter paper represents the total suspended solids.
Interference: Large floating particles or submerged agglomerates of non-homogeneous material should be excluded from the sample. Because excessive residue on the filter paper may form water-entrapping crust, sample size should be limited to that yielding no more than 200g residue.
APPARATUS
- · Beaker
- · Measuring cylinder
- · Drying oven
- · Weighing balance
- · Filter paper
- · Desiccator
PROCEDURES INVOLVES
- Dry a filter paper to a constant weight at 103oC to 105oC in an oven
- Weigh the dried filter paper
- Filter 100ml of the sample through the dried filter paper
- Carefully transfer the filter paper containing the suspended solids to the oven and dry at 103oC to 105oC for about 15mins
- Take the filter paper to a desiccator and cool
- Weigh the cooled filter paper
- Repeat drying, cooling and weighing until weight loss is less than 4% of previous weight
CALCULATION
Mg
total suspended solid per liter = (A – B) x 1000
Sample volume, ml
Where: A =
weight of filter + dried residue, mg.
B = weight of filter, mg.
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