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Thursday 8 March 2018

TOTAL SUSPENDED SOLIDS (TSS)



TOTAL SUSPENDED SOLIDS (TSS)

Principle :A well-mixed sample is filtered through a weighed standard filter paper and dried to a constant weight at 103oC to 105oC.The increase in weight of the filter paper represents the total suspended solids.


Interference: Large floating particles or submerged agglomerates of non-homogeneous material should be excluded from the sample. Because excessive residue on the filter paper may form water-entrapping crust, sample size should be limited to that yielding no more than 200g residue.


APPARATUS
  • ·           Beaker
  • ·        Measuring cylinder
  • ·        Drying oven
  • ·        Weighing balance
  • ·        Filter paper
  • ·        Desiccator

PROCEDURES INVOLVES
  •         Dry a filter paper to a constant weight at 103oC to 105oC in an oven
  •         Weigh the dried filter paper
  •         Filter 100ml of the sample through the dried filter paper
  •        Carefully transfer the filter paper containing the suspended solids to the oven and dry at 103oC to 105oC for about 15mins
  •        Take the filter paper to a desiccator and cool
  •        Weigh the cooled filter paper
  •         Repeat drying, cooling and weighing until weight loss is less than 4% of previous weight

CALCULATION
Mg total suspended solid per liter     =       (A – B) x 1000
                                                                  Sample volume, ml
Where:        A       = weight of filter + dried residue, mg.
                   B       = weight of filter, mg.

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